HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54559713, compound → HCID 14576184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54559713 | HCID 54559713 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14576184 | HCID 14576184 | — |
Reaction Steps
A solution of the compound of Example 29 (0.90 g, 2.7 mmol) in ethyl acetate (100 ml) was treated with platinum oxide (0.4 g) and reduced for 3 hours at atmospheric pressure. The catalyst was filtered, the filtrate evaporated and the residue (0.87 g) was crystallized from hexane to yield the title compound, m.p. 39°-40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851425 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-f691e64905ab4a76be3dfd9c634c9884 |
| Source note | uspto-grants-1989_07 |