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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 232144Generated: October 28, 2026

HCID 54559713, compound → HCID 14576184, compound

https://huagongshe.com/reaction/232144

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54559713HCID 54559713—
CatalystPlatinum oxide (PtO)HCID 82844—
SolventEthyl AcetateHCID 8857—
ProductHCID 14576184HCID 14576184—

Reaction Steps

A solution of the compound of Example 29 (0.90 g, 2.7 mmol) in ethyl acetate (100 ml) was treated with platinum oxide (0.4 g) and reduced for 3 hours at atmospheric pressure. The catalyst was filtered, the filtrate evaporated and the residue (0.87 g) was crystallized from hexane to yield the title compound, m.p. 39°-40° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04851425
Source datasetuspto-grants-1989_07
ORD IDord-f691e64905ab4a76be3dfd9c634c9884
Source noteuspto-grants-1989_07