HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20030930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 86743267 | HCID 86743267 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 20030930 | HCID 20030930 | — |
Reaction Steps
In 15 ml of dichloroethane was dissolved 580 mg of Compound (97), followed by addition of 0.58 ml of thionyl chloride. The mixture was heated for one hour under reflux. The solvent was evaporated off, and the residue was treated with isopropylether to give 500 mg of the subject Compound (98) as colorless crystals, m.p. 132°-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851422 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-89123cdad9c847ea8d5509cddc926a77 |
| Source note | uspto-grants-1989_07 |