HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Oxabicyclo(3.1.0)hexane-2,4-dione → HCID 20031396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Oxabicyclo(3.1.0)hexane-2,4-dione | HCID 2734721 | — |
| Reactant | 1-pentylpiperazine | HCID 2737112 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20031396 | HCID 20031396 | — |
Reaction Steps
To 100 mL of ethanol is added 1-pentylpiperazine (15.6 g, 0.1 mol) and 11.2 g (0.1 mol) of 3-oxabicyclo[3.1.0]-hexane-2,4-dione. Reflux the reaction and monitor by thin-layer chromatography. Upon completion remove the solvent in vacuo to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851526 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-0fe2c3b1dd8f4652ac9d496cae8f9b31 |
| Source note | uspto-grants-1989_07 |