HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 14555604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Glyoxal | HCID 7860 | — |
| Reactant | HCID 14555603 | HCID 14555603 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 14555604 | HCID 14555604 | — |
Reaction Steps
A mixture of 25.4 g (0.1 mol) of 4-[1-methyl-3-(morpholin-4-yl)propoxy]benzenamine, 6.8 g of 25% aqueous ammonia, and 10 mL of 2-propanol, and a mixture of 5.8 (0.1 mol) of glyoxal and 7.5 (0.1 mol) of 40% aqueous formaldehyde are simultaneously added into 20 mL of 1-propanol in the course of 30 minutes at 80° C. Monitor the reaction by thin-layer chromatography. Upon completion remove the solvent in vacuo to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851526 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-4fa1e59688b143c9b78d8b058eef37fc |
| Source note | uspto-grants-1989_07 |