HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxybenzoyl chloride → 4-Cyano-3-(2-ethoxybenzylamino)pyridine-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxybenzoyl chloride | HCID 3016397 | — |
| Reactant | 3-Amino-4-cyanopyridine-2-carboxamide | HCID 22462404 | — |
| Product | 4-Cyano-3-(2-ethoxybenzylamino)pyridine-2-carboxamide | HCID 23358990 | — |
Reaction Steps
The title compound was prepared from 2-ethoxybenzoyl chloride and 3-amino-4-cyanopyridine-2-carboxamide (Preparation 12), following the procedure of Preparation 7, and was obtained as a colourless solid. (6.2%), m.p. 150°-152° C. Found: C,61.99; H,4.62; N,17.84. C16H14N4O3 requires C,61.93; H,4.55; N,18.06%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591742 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-35681905909448cfb407157f4d6fb33b |
| Source note | uspto-grants-1997_01 |