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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 232725Generated: October 26, 2026

(+-)-2-Butanol → (1-Methylpropoxycarbonyl)sulfenyl chloride

https://huagongshe.com/reaction/232725

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(+-)-2-ButanolHCID 6568—
Reactant(Chlorothio)formyl chlorideHCID 75990—
Product(1-Methylpropoxycarbonyl)sulfenyl chlorideHCID 1363329039.1%

Reaction Steps

Chlorocarbonylsulfenyl chloride (13.1 g, 0.1 mol) was mixed with 2-butanol (6.7 g, 0.09 mol)and warmed to about 35° to 40° C. for one hour. Distillation resulted in the tithe compound (5.93 g) Bp. 70° C./0.8 mm Hg. NMR spectrum was consistent with the structure.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05591764
Source datasetuspto-grants-1997_01
ORD IDord-61cd90b086e14eeaa59c139b8c8dc5ed
Source noteuspto-grants-1997_01