HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → 1-(2-Ethyl-4-methylimidazolylmethyl)-2-naphthol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 2-Naphthol | HCID 8663 | — |
| Reactant | HCID 178437635 | HCID 178437635 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 1-(2-Ethyl-4-methylimidazolylmethyl)-2-naphthol | HCID 178437614 | 85% |
Reaction Steps
To a 35% solution of 2-ethyl-4-methylimidazole (110g, 1 mole) and 2-naphthol (144 g, 1 mole) in isopropanol, formaline (37% aqueous solution, 1 mole of CH2O) is added over a period of 15 minutes at room temperature, followed by three hours of refluxing at 82°-84° C. The product (a white powder) is obtained in a yield of 85%, with a melting point of 166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591811 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-738efcbc3eb245419d2f0d76fb30580d |
| Source note | uspto-grants-1997_01 |