HRID232815

反应详情

EQUATION

反应方程式

HRID 232815 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a 35% solution of 2-ethyl-4-methylimidazole (110g, 1 mole) and 2-naphthol (144 g, 1 mole) in isopropanol, formaline (37% aqueous solution, 1 mole of CH2O) is added over a period of 15 minutes at room temperature, followed by three hours of refluxing at 82°-84° C. The product (a white powder) is obtained in a yield of 85%, with a melting point of 166° C.

WORKUP

后处理

  1. temperatureof refluxing at 82°-84° C
  2. customThe product (a white powder) is obtained in a yield of 85%, with a melting point of 166° C.