HRID232815
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a 35% solution of 2-ethyl-4-methylimidazole (110g, 1 mole) and 2-naphthol (144 g, 1 mole) in isopropanol, formaline (37% aqueous solution, 1 mole of CH2O) is added over a period of 15 minutes at room temperature, followed by three hours of refluxing at 82°-84° C. The product (a white powder) is obtained in a yield of 85%, with a melting point of 166° C.
WORKUP
后处理
- temperatureof refluxing at 82°-84° C
- customThe product (a white powder) is obtained in a yield of 85%, with a melting point of 166° C.