HRID232820
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
3.6 g of methyl 2-aminoindane-5-acetatehydrochloride are refluxed for 3 hours in 160 ml of semiconcentrated hydrochloric acid. The hydrochloric acid is distilled off and the remaining product is triturated with a little ethanol, suction filtered and dried in vacuo.
WORKUP
后处理
- distillationThe hydrochloric acid is distilled off
- customthe remaining product is triturated with a little ethanol, suction
- filtrationfiltered
- customdried in vacuo