HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54008131, compound → HCID 54425397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54008131 | HCID 54008131 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54425397 | HCID 54425397 | 96% |
Reaction Steps
A solution of ethyl 2-(N-benzyloxycarbonyl-N-methylaminoacetylamino)tetralin-2-carboxylate (750 mg, 1.8 mmol) in ethanol (20 ml) was subjected to hydrogenation in the presence of 10% palladium-carbon (200 mg) for 5 hours. After the catalyst was filtered off, the mother liquid was concentrated under reduced pressure to yield 500 mg (96%) of the title compound as a crude substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591849 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-5e3c247104b145368049a7d6c9840a12 |
| Source note | uspto-grants-1997_01 |