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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 232888Generated: October 31, 2026

HCID 54008131, compound → HCID 54425397, compound

https://huagongshe.com/reaction/232888

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54008131HCID 54008131—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 54425397HCID 5442539796%

Reaction Steps

A solution of ethyl 2-(N-benzyloxycarbonyl-N-methylaminoacetylamino)tetralin-2-carboxylate (750 mg, 1.8 mmol) in ethanol (20 ml) was subjected to hydrogenation in the presence of 10% palladium-carbon (200 mg) for 5 hours. After the catalyst was filtered off, the mother liquid was concentrated under reduced pressure to yield 500 mg (96%) of the title compound as a crude substance.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05591849
Source datasetuspto-grants-1997_01
ORD IDord-5e3c247104b145368049a7d6c9840a12
Source noteuspto-grants-1997_01