HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-chloropyridine-2-carbonitrile → HCID 131724730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-chloropyridine-2-carbonitrile | HCID 22591246 | — |
| Reactant | Tert-butyl (7br,11as)-6-amino-1,2,7b,10,11,11a-hexahydro-4h-[1,4]oxazepino[6,5,4-hi]pyrido[4,3-b]indole-9(8h)carboxylate | HCID 86586438 | — |
| Product | HCID 131724730 | HCID 131724730 | — |
Reaction Steps
Following the procedures described in Example 176 and using 3-bromo-5-chloro-2-cyanopyridine, tert-butyl (7bR,11aS)6-amino-1,2,7b,10,11,11a-hexahydro-4H-[1,4]oxazepino[6,5,4-hi]pyrido[4,3-b]indole-9(8H)-carboxylate from Example 56, Part B was converted into the title compound of Example 177. ESI MS m/z 382.3/384.3 [C20H20CIN5O+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849619B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-ccc3b24ca0b6486588acb2b76709b7ed |
| Source note | uspto-grants-2005_02 |