Dimethylformamide → 2,4-Bis(dichloromethylidene)-2H,4H-1,3-benzodioxine-6-carbonitrile

HRID 2331026Notes

Reaction equation

HRID 2331026 reaction equation
[CH3:24][N:25]([CH3:26])[CH:27]=[O:28].[Cl:1][C:2](=[C:3]1[O:4][c:5]2[c:6]([cH:12][c:13]([C:16](=[O:17])[NH2:18])[cH:14][cH:15]2)[C:7](=[C:9]([Cl:10])[Cl:11])[O:8]1)[Cl:19].[S:20]([Cl:21])([Cl:22])=[O:23]>>[Cl:1][C:2](=[C:3]1[O:4][c:5]2[c:6]([cH:12][c:13]([C:16]#[N:18])[cH:14][cH:15]2)[C:7](=[C:9]([Cl:10])[Cl:11])[O:8]1)[Cl:19]

Participants

4

Reactant 3

HCID 6228DimethylformamideHCID 24386Thionyl ChlorideHCID 233329192,4-Bis(dichloromethylidene)-2H,4H-1,3-benzodioxine-6-carboxamide

Product 1

HCID 233329162,4-Bis(dichloromethylidene)-2H,4H-1,3-benzodioxine-6-carbonitrile

Sources & evidence

ORD record
ord-c8d6fc0ae4ea4399b27b4d19b61da190
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (10/10)

Reaction notes

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