HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9887252, compound → HCID 23361334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9887252 | HCID 9887252 | — |
| Reactant | 4-((5,6,7,8-Tetrahydro-8,8-dimethyl-5-oxonaphth-2-yl)ethynyl]benzoic acid | HCID 15345547 | — |
| Product | HCID 23361334 | HCID 23361334 | — |
Reaction Steps
Employing the same general procedure as for the preparation of 4-[(5,6,7,8-tetrahydro-8,8-dimethyl-5-oxonaphth-2-yl)ethynyl]benzoic acid (Compound 7), 90 mg (0.23 mmol) of ethyl 4-[(7,8-dihydro-8,8-dimethyl-5(6H)-(3-pentylidene)naphth-2-yl)ethynyl]benzoate (Compound 133) was converted to the title compound using 0.5 ml (0.5 mmol) of LiOH (1M aqueuos solution).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591858 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-d34cba50ddc443949007dec95b93bacc |
| Source note | uspto-grants-1997_01 |