HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 23361375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | HCID 23361347 | HCID 23361347 | — |
| Product | HCID 23361375 | HCID 23361375 | — |
Reaction Steps
According to the method described for Reference Example 25, 5-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-1-pentanol was allowed to react with phosphorus tribromide to give 5-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]pentyl bromide. Recrystallization from ether-hexane gave colorless needles, m.p.58°-59° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-96ecebd4cefb4b9f870e67a2f7d6d2d5 |
| Source note | uspto-grants-1997_01 |