HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl phosphonoacetate → HCID 86754595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl phosphonoacetate | HCID 80029 | — |
| Reactant | HCID 10638429 | HCID 10638429 | — |
| Product | HCID 86754595 | HCID 86754595 | — |
Reaction Steps
According to the method described for Reference Example 22, 4'-(5-methyl-2-phenyl-4-oxazolylmethoxy)acetophenone was allowed to react with trimethyl phosphonoacetate gave methyl (E)-3-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-butenoate. Recrystallization from ethyl acetate--hexane gave colorless prisms, m.p.125°-126° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-9469f0de31264fdaa1c97f930222d415 |
| Source note | uspto-grants-1997_01 |