HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → 4-[5-Methyl-2-(2-naphthyl)-4-oxazolylmethoxy]benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | 4-(Chloromethyl)-5-methyl-2-(naphthalen-2-yl)-1,3-oxazole | HCID 12158073 | — |
| Product | 4-[5-Methyl-2-(2-naphthyl)-4-oxazolylmethoxy]benzaldehyde | HCID 18546159 | — |
Reaction Steps
According to the method described for Reference Example 45, 4-chloromethyl-5-methyl-2-(2-naphthyl)oxazole was allowed to react with p-hydroxybenzaldehyde to give 4-[5-methyl-2-(2-naphthyl)-4-oxazolylmethoxy]benzaldehyde. Recrystallization from chloroform-ether gave colorless prisms, m.p.163°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-c9e016b07ed549308a2ff9198fdbd080 |
| Source note | uspto-grants-1997_01 |