HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (cyanomethyl)phosphonate → HCID 54037696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (cyanomethyl)phosphonate | HCID 75676 | — |
| Reactant | HCID 23361370 | HCID 23361370 | — |
| Product | HCID 54037696 | HCID 54037696 | — |
Reaction Steps
According to the method described for Reference Example 35, 4-[3-(5-methyl-2-phenyl-4-oxazolyl)propoxy]benzaldehyde was allowed to react with diethyl cyanomethylphosphonate to give 4-[3-(5-methyl-2-phenyl-4-oxazolyl)propoxy]cinnamonitrile. Recrystallization from ethyl acetate--isopropyl ether--hexane gave colorless prisms, m.p.97°-98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-6ecbf345ac714cee9f324d66c4de0acc |
| Source note | uspto-grants-1997_01 |