Hydrochloric Acid → HCID 357793, compound

HRID 233345Notes

Reaction equation

HRID 233345 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].Cl.[CH3:12]O>>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([O:10][CH3:12])=[O:9]

Participants

4

Procedure

6-Methoxy-caproic acid (6.17 g) was dissolved in dry methanol (90 ml) containing hydrogen chloride (catalytic amount) and held overnight at room temperature. The solvent was distilled off from the reaction solution under reduced pressure to give methyl 6-methoxy-caproate. Yield; 5.68 g

Workup

  1. distillationThe solvent was distilled off from the reaction solution under reduced pressure

Sources & evidence

ORD record
ord-3bf6b8ce0af84ca584f86c1583ab0cc8
Source dataset
uspto-grants-1997_01
Patent number
US05591887

Reaction notes

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