HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzaldehyde → HCID 54065590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzaldehyde | HCID 68009 | — |
| Reactant | diethoxyphosphoryl-phenyl-methanol | HCID 238674 | — |
| Product | HCID 54065590 | HCID 54065590 | 79% |
Reaction Steps
The procedure described for the preparation of Compound 19 is used except that 3-fluorobenzaldehyde (1.49 g, 0.012M) is used in place of benzaldehyde. The solid obtained is recrystallized from hexane to obtain 2.474 g (0.009 M, 79%) of colorless short needles: mp 81°-82° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05593980 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-f247d4a486114a768a94fa69919af3f3 |
| Source note | uspto-grants-1997_01 |