Dichloromethane → Tert-butyl 4-(dibromomethylene)piperidine-1-carboxylate

HRID 2335893Notes

Reaction equation

HRID 2335893 reaction equation
[C:20]([Br:21])([Br:22])([Br:23])[Br:24].[Cl:39][CH2:40][Cl:41].[O:25]=[C:26]1[CH2:27][CH2:28][N:29]([C:32](=[O:33])[O:34][C:35]([CH3:36])([CH3:37])[CH3:38])[CH2:30][CH2:31]1.[c:1]1([P:2]([c:3]2[cH:4][cH:5][cH:6][cH:7][cH:8]2)[c:9]2[cH:10][cH:11][cH:12][cH:13][cH:14]2)[cH:15][cH:16][cH:17][cH:18][cH:19]1>>[C:20]([Br:21])([Br:24])=[C:26]1[CH2:27][CH2:28][N:29]([C:32](=[O:33])[O:34][C:35]([CH3:36])([CH3:37])[CH3:38])[CH2:30][CH2:31]1

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 11205Carbon tetrabromideHCID 11776TriphenylphosphineHCID 735900tert-Butyl 4-oxopiperidine-1-carboxylate

Product 1

HCID 53486134Tert-butyl 4-(dibromomethylene)piperidine-1-carboxylate

Sources & evidence

ORD record
ord-2a003a11c8a441368de4ba5e23693149
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (10/10)

Reaction notes

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