Potassium Bromide → HCID 54426699, compound

HRID 233633Notes

Reaction equation

HRID 233633 reaction equation
[CH3:1][C:2]([C:18]([NH:20][CH2:21][C:22]12[CH2:31][CH:26]3[CH2:27][CH:28]([CH2:30][CH:24]([CH2:25]3)[CH2:23]1)[CH2:29]2)=[O:19])([CH2:8][C:9]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[NH:11][CH:10]=1)[C:3]([O:5]CC)=[O:4].CC(C(NC1C2CC3CC(CC1C3)C2)=O)(CC1C2C(=CC=CC=2)NC=1)C(O)=O.[K+].[Br-]>>[CH3:1][C:2]([C:18]([NH:20][CH2:21][C:22]12[CH2:31][CH:26]3[CH2:27][CH:28]([CH2:30][CH:24]([CH2:25]3)[CH2:23]1)[CH2:29]2)=[O:19])([CH2:8][C:9]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[NH:11][CH:10]=1)[C:3]([OH:5])=[O:4]

Participants

4

Reactant 3

HCID 253877Potassium BromideHCID 53831131HCID 53831131, compound2×HCID 54178673HCID 54178673, compound

Product 1

HCID 54426699HCID 54426699, compound

Procedure

Compound 10 was prepared from Compound 9 according to the procedure for Compound 6. The product was obtained as a white solid. 1.95 9 (71%) IR (KBr) 3440, 2912, 1713, 1652, 1621, 1189, 746 cm-1.

Workup

  1. customThe product was obtained as a white solid

Sources & evidence

ORD record
ord-2913f78a8ad9426082b331b100d71646
Source dataset
uspto-grants-1997_01
Patent number
US05593967

Reaction notes

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