Hydrochloric Acid → HCID 14857732, compound

HRID 233635Notes

Reaction equation

HRID 233635 reaction equation
[ClH:1].[NH2:2][CH:3]1[C:11]2[C:6](=[CH:7][C:8]([O:12][CH3:13])=[CH:9][CH:10]=2)[C:5]([CH3:19])([CH2:14][C:15]([O:17]C)=[O:16])[CH2:4]1.Cl>>[ClH:1].[NH2:2][CH:3]1[C:11]2[C:6](=[CH:7][C:8]([O:12][CH3:13])=[CH:9][CH:10]=2)[C:5]([CH3:19])([CH2:14][C:15]([OH:17])=[O:16])[CH2:4]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 14857731HCID 14857731, compound

Product 1

HCID 14857732HCID 14857732, compoundYield 97.3%

Procedure

4 g of the title compound of Example 2 in 2 normal hydrochloric acid was heated to reflux, stirred at that temperature for 3 hours and evaporated to give 3.7 g of white solid.

Workup

  1. temperatureto reflux
  2. customevaporated

Sources & evidence

ORD record
ord-fcfbacda94e34688bc2abfb5d127d68b
Source dataset
uspto-grants-1997_01
Patent number
US05594002

Reaction notes

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