Maleic Acid → HCID 131717124, compound

HRID 233660Notes

Reaction equation

HRID 233660 reaction equation
[CH3:1][N:2]1[CH2:13][CH2:12][C:5]2([O:9][CH2:8][C:7](=[N:10][OH:11])[CH2:6]2)[CH2:4][CH2:3]1.[C:14]([OH:21])(=[O:20])/[CH:15]=[CH:16]\[C:17]([OH:19])=[O:18]>C(OCC)(=O)C>[C:14]([OH:21])(=[O:20])/[CH:15]=[CH:16]\[C:17]([OH:19])=[O:18].[CH3:1][N:2]1[CH2:13][CH2:12][C:5]2([O:9][CH2:8][C:7](=[N:10][OH:11])[CH2:6]2)[CH2:4][CH2:3]1

Participants

4

Reactant 2

HCID 444266Maleic AcidHCID 72742956HCID 72742956, compound

Product 1

HCID 131717124HCID 131717124, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The compound of Example 3 (0.76 g, 4.1 mmol) was dissolved in hot ethyl acetate and mixed with maleic acid (0.48 g, 0.41 mmol) to give the title compound as a white solid, mp 183°-184°.

Sources & evidence

ORD record
ord-fcc2353b2a774bbb97216ce539e51cc2
Source dataset
uspto-grants-1997_01
Patent number
US05594000

Reaction notes

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