HRID23382

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CS(=O)(=O)c1cn(CC2=NCCN2)c2ccc([N+](=O)[O-])cc12

HCID22574065

未命名化合物

PRODUCTS

生成物

结构：CS(=O)(=O)c1cn(CC2=NCCN2)c2ccc(N)cc12

HCID22574067

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

1-(4,5-Dihydro-1H-imidazol-2-ylmethyl)-3-methanesulfonyl-1H-indol-5-ylamine, (mp 215-217° C.) was prepared by reduction of the nitro group of compound 1-(4,5-dihydro-1H-imidazol-2-ylmethyl)-3-methanesulfonyl-5-nitro-1H-indole, with TiCl3 in aqueous acetonitrile.