HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 11122592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | (+)-Boldine | HCID 10154 | — |
| Product | HCID 11122592 | HCID 11122592 | — |
Reaction Steps
1 g of boldine was dissolved in 30 ml of (DMF), the mixture was reacted with 1.2 ml of benzyl chloride at 100°-110° C. for 2 hrs. The residue obtained after evaporation under reduced pressure was purified to give the pure compound (5) N-benzylsecoboldine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05594033 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-a5735dddb0d24067a369730333bf50a7 |
| Source note | uspto-grants-1997_01 |