Sodium Azide → HCID 178441447, compound

HRID 233972Notes

Reaction equation

HRID 233972 reaction equation
[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:23]#[N:24])=[CH:13][CH:12]=2)[C:8]2[CH:25]=[C:26]([C:29]3[N:30]=[C:31]4[CH:36]=[CH:35][CH:34]=[CH:33][N:32]4[CH:37]=3)[CH:27]=[CH:28][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4].[N-:38]=[N+:39]=[N-:40].[Na+]>CN(C)C=O>[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:12]=[CH:13][C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:23]3[NH:40][N:39]=[N:38][N:24]=3)=[CH:15][CH:16]=2)[C:8]2[CH:25]=[C:26]([C:29]3[N:30]=[C:31]4[CH:36]=[CH:35][CH:34]=[CH:33][N:32]4[CH:37]=3)[CH:27]=[CH:28][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 33557Sodium AzideHCID 19965041HCID 19965041, compound

Product 1

HCID 178441447HCID 178441447, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared analogously to Example 10 from 4'-[[2-n-butyl-6-(imidazo[1,2-a]pyridin-2-yl)-benzimidazol-1-yl]-methyl]-2-cyano-biphenyl and sodium azide in dimethylformamide.

Sources & evidence

ORD record
ord-a9add4712bb54b5291ff80bf2caeac17
Source dataset
uspto-grants-1997_01
Patent number
US05594003

Reaction notes

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