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HRID234348

反应详情

EQUATION

反应方程式

HRID 234348 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：O=S(=O)(Cl)Cl
HCID24648

Sulfuryl chloride

Cl2O2S

结构：c1ccc2sc(Cc3ccc4c(c3)OCO4)cc2c1
HCID22998407

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(Cl)c1c(Cc2ccc3c(c2)OCO3)sc2ccccc12
HCID22998385

未命名化合物

PROCEDURE

实验过程

2-[3,4-(methylenedioxy)benzyl]benzo[b]thiophene-3-sulfonyl chloride was prepared by the method of Example 40B using DMF (9.1 mmoles, 0.70 ml), sulfuryl chloride (7.7 mmoles, 0.62 ml) and 2-[3,4-(methylenedioxy)benzyl]benzo[b]thiophene (4.6 mmoles, 1.2 g). Flash chromatography (5% ethyl acetate/hexanes) provided 0.71 g (42%) of a light yellow solid.