HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethoxybenzenesulfonyl chloride → HCID 19076474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethoxybenzenesulfonyl chloride | HCID 2734626 | — |
| Reactant | HCID 19076611 | HCID 19076611 | — |
| Product | HCID 19076474 | HCID 19076474 | — |
Reaction Steps
This compound is prepared according to the procedure described in EXAMPLE 1 from 0.500 g of 5-ethoxy-3-(2-ethoxycarbonyl-1-ethoxycarbonylhydrazino)-1,3-dihydro-3-phenylindol-2-one and 0.280 g of 2,4-dimethoxybenzenesulfonyl chloride. The expected product is obtained after crystallization from a DCM/iso ether mixture. m=0.383 g. M.p.=228°-229° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05594023 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-7b951e58becb46c1833cff2ea6c8b40c |
| Source note | uspto-grants-1997_01 |