HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 1-Bromo-2-fluoro-4-tridecyloxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Bromotridecane | HCID 13000 | — |
| Reactant | 4-Bromo-3-fluorophenol | HCID 2779153 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | 1-Bromo-2-fluoro-4-tridecyloxybenzene | HCID 23354725 | — |
Reaction Steps
This was prepared using a similar method to that described for compound 3. Quantities: compound 1 (4.02 g, 21.1 mmol), 1-bromotridecane (6.11 g, 23.2 mmol), potassium carbonate (5.22 g, 37.8 mmol) and butanone (115 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05595682 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-b754ed3169634929b3e30f44e30db084 |
| Source note | uspto-grants-1997_01 |