4-Cyanobenzoic acid → HCID 178447783, compound

HRID 234563Notes

Reaction equation

HRID 234563 reaction equation
[C:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1)#[N:2].[C:12]1([Si:18]2(CCCCC)[CH2:23][CH2:22][CH:21]([SiH:24]3[CH2:29][CH2:28][CH:27](O)[CH2:26][CH2:25]3)[CH2:20][CH2:19]2)C=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7]([O:9][C@H:27]2[CH2:28][CH2:29][Si@H:24]([CH:21]3[CH2:22][CH2:23][SiH:18]([CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[CH2:19][CH2:20]3)[CH2:25][CH2:26]2)=[O:8])=[CH:5][CH:4]=1)#[N:2]

Participants

3

Reactant 2

HCID 120874-Cyanobenzoic acidHCID 123959416HCID 123959416, compound

Product 1

HCID 178447783HCID 178447783, compound

Procedure

The general procedure of Example 31 was repeated using 4-cyanobenzoic acid and 4-(4-phenyl-4-n-pentyl-4-silacyclohexyl)-4-silacyclohexanol, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-c2a21c852215411da7164584374845e3
Source dataset
uspto-grants-1997_01
Patent number
US05595686

Reaction notes

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