HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,7-Dichloroquinoline → HCID 9947937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,7-Dichloroquinoline | HCID 6866 | — |
| Reactant | N-(2-Aminoethyl)piperidine | HCID 33944 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 9947937 | HCID 9947937 | — |
Reaction Steps
3.57 g of base from 3.96 g of 4,7-dichloroquinoline and 4.8 g of 1-(2-aminoethyl)-piperidine (reaction duration, 5 hours at 140° C.); yellowish crystals from acetonitrile, m.p.: 148°-151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05596002 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-ba5f98369f4f45d9a305cc64cc876d1e |
| Source note | uspto-grants-1997_01 |