4,7-Dichloroquinoline → HCID 53891666, compound

HRID 234685Notes

Reaction equation

HRID 234685 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][C:8]([Cl:12])=[CH:9][CH:10]=2)[N:5]=[CH:4][CH:3]=1.[CH3:13][N:14]([CH2:16][CH2:17][CH2:18][NH2:19])[CH3:15]>C(OCC)(=O)C.CCCCCC>[Cl:12][C:8]1[CH:7]=[C:6]2[C:11]([C:2]([CH:16]([N:14]([CH3:15])[CH3:13])[CH2:17][CH2:18][NH2:19])=[CH:3][CH:4]=[N:5]2)=[CH:10][CH:9]=1

Participants

4

Reactant 2

HCID 68664,7-DichloroquinolineHCID 7993N,N-Dimethyl-1,3-propanediamine

Product 1

HCID 53891666HCID 53891666, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

From 4,7-dichloroquinoline and 3-(N,N-dimethylamino)-propylamine; colourless crystals from ethyl acetate-hexane, m.p.: 111°-113° C.

Sources & evidence

ORD record
ord-15b6fe7e2cd942eeb737a35716692c08
Source dataset
uspto-grants-1997_01
Patent number
US05596002

Reaction notes

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