HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 10379653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14257839 | HCID 14257839 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10379653 | HCID 10379653 | — |
Reaction Steps
Mix phenyl[1-(2-phenylethyl)-4-piperidinyl]methanone·HCl (5.0g, 15.16mmol), 1N sodium hydroxide (100mL) and methylene chloride (250mL) and stir overnight at room temperature. Separate the organic phase and extract the aqueous phase with methylene chloride. Combine the organic phases, dry (MgSO4) and evaporate the solvent in vacuo to give phenyl[1-(2-phenylethyl)-4-piperidinyl]methanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05596003 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-d9612964958141759866b83a38c87061 |
| Source note | uspto-grants-1997_01 |