Diphenylamine → HCID 86750223, compound

HRID 234714Notes

Reaction equation

[C:1]1([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH:14][CH2:15][CH2:16][CH2:17][CH:18]1[C:27]2[C:22](=[C:23]([O:28][CH2:29][C:30]([O:32][CH3:33])=[O:31])[CH:24]=[CH:25][CH:26]=2)[CH2:21][CH2:20][CH2:19]1>>[C:8]1([N:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[C:15]([CH2:16][CH2:17][CH:18]2[C:27]3[C:22](=[C:23]([O:28][CH2:29][C:30]([O:32][CH3:33])=[O:31])[CH:24]=[CH:25][CH:26]=3)[CH2:21][CH2:20][CH2:19]2)=[O:14])[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

Participants

Reactant 2

HCID 11487Diphenylamine

HCID 15238044HCID 15238044, compound

Product 1

HCID 86750223HCID 86750223, compound

Procedure

By the same procedure as reference example 1→reference example 2→example 1 (using diphenylamine instead of dibenzylamine), using methyl [1-(3-hydroxypropyl)-1,2,3,4-tetrahydronaphthalen-5-yl]oxyacetate instead of methyl(1-hydroxymethyl-1,2,3,4-tetrahydronaphthalen-5-yl)oxyacetate, was obtained methyl [1-(2-diphenylaminocarbonylethyl)-1,2,3,4-tetrahydronaphthalen-5-yl]oxyacetate. By the same procedure as example 2, using methyl [1-(2-diphenylaminocarbonylethyl)-1,2,3,4-tetrahydronaphtahalen-5-yl]oxyacetate thus obtained, the title compound having the following physical data was given.

Sources & evidence

ORD record: ord-052335562fcc45b6a94a73acf4eb048b
Source dataset: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05596009

Reaction notes

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