HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86750229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-trityl-1-[4-(benzoxazol-2-yl)benzyloxy]tricyclo[3.3.1.13,7]-decan-2-amine | HCID 54303745 | — |
| Product | HCID 86750229 | HCID 86750229 | — |
Reaction Steps
N-trityl-1-[4-(benzoxazol-2-yl)benzyloxy]tricyclo[3.3.1.13,7 ]-decan-2-amine (0.88 g; 0.0014 mole) is combined with ethanolic HCl (20 ml). After 2 hours, TLC indicates the reaction is complete. The reaction mixture is evaporated to dryness and purified on a flash column, using 10% MeOH/CH2Cl2 to obtain 1-[4-(benzoxazol-2-yl)benzyloxy]-tricyclo[3.3.1.13,7 ]-decan-2-amine hydrochloride (m.p. 291°-293° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05596020 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-932d53a90ec640948c5776398fcf5c68 |
| Source note | uspto-grants-1997_01 |