Benzyl Alcohol → HCID 86750241, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 1.6 g of 4-amidino-4'-[(4-carbonylmethylpiperidino)carbonyl]biphenyl hydrochloride, 50 ml of benzyl alcohol and 1 g of p-toluenesulphonic acid is heated to 70° C. with stirring for 4 hours under 100 mbar and then evaporated down in a water jet vacuum at 140°-150° C. The residue was triturated with ether, the solid product obtained was filtered off and dissolved in dimethylformamide, the solution was evaporated down and the residue was triturated with ether.

Provenance & Evidence