m-Chloroperbenzoic acid → HCID 53897772, compound

HRID 234983Notes

Reaction equation

HRID 234983 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:15]=[CH:14][C:13]([S:16][CH2:17][CH2:18][CH2:19][CH2:20][C:21]([O:23][CH3:24])=[O:22])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)(=[NH:3])[NH2:2].ClC1C=CC=C(C(OO)=[O:33])C=1>C(Cl)Cl>[C:1]([C:4]1[CH:5]=[CH:6][C:7]([C:10]2[CH:15]=[CH:14][C:13]([S:16]([CH2:17][CH2:18][CH2:19][CH2:20][C:21]([O:23][CH3:24])=[O:22])=[O:33])=[CH:12][CH:11]=2)=[CH:8][CH:9]=1)(=[NH:2])[NH2:3]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 54555066HCID 54555066, compound

Product 1

HCID 53897772HCID 53897772, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Prepared from 4-amidino-4'-(4-methoxycarbonylbutylthio)biphenyl by oxidation with m-chloro-perbenzoic acid in methylene chloride at -20° C. for 15 hours.

Sources & evidence

ORD record
ord-352b0bc3a07f4b39ad42972191e95d99
Source dataset
uspto-grants-1997_01
Patent number
US05597825

Reaction notes

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