m-Chloroperbenzoic acid → HCID 178508838, compound

HRID 235014Notes

Reaction equation

HRID 235014 reaction equation
Cl.[NH2:2][C:3]1[N:8]=[C:7]([NH2:9])[C:6]([C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([Cl:16])[C:11]=2[Cl:17])=[C:5]([C:18]([F:21])([F:20])[F:19])[N:4]=1.C1C=C(Cl)C=C(C(OO)=[O:30])C=1>C(Cl)(Cl)Cl>[NH2:2][C:3]1[N:8]=[C:7]([NH2:9])[C:6]([C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([Cl:16])[C:11]=2[Cl:17])=[C:5]([C:18]([F:21])([F:20])[F:19])[N+:4]=1[O-:30]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 197050922,4-Diamino-5-(2,3-dichlorophenyl)-6-trifluoromethylpyrimidine hydrochloride

Product 1

HCID 178508838HCID 178508838, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

This compound was made from the compound of Example 14 by reaction with MCPBA in CHCl3 at room temperature. Mp. 275°-278° C.

Sources & evidence

ORD record
ord-c9997357ab7a4f4980540637f7df3494
Source dataset
uspto-grants-1997_01
Patent number
US05597828

Reaction notes

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