HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53663285, compound → 88467-55-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53663285 | HCID 53663285 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 88467-55-4 | HCID 13588493 | 70% |
Reaction Steps
This was prepared from compound (1) in 70% yield by hydrogenation over platinum oxide in glacial acetic acid: b.p. 67°-70° C. at 8.5 mm; NMR (CDCl3) 0.86 (t, CH3CH2), 0.87 (d, CH3CH), 3.40 (m, 2H, CH2CH2Br)). The IR and NMR spectra of the compound were in complete agreement with the assigned structure and reported values.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04871537 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-507a8b6f74524016a9c0d5e586da26b5 |
| Source note | uspto-grants-1989_10 |