HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → 3,6-Di(p-nitrostyryl)pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | 3,6-Dimethylpyridazine | HCID 527031 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | 3,6-Di(p-nitrostyryl)pyridazine | HCID 54059565 | 44.4% |
Reaction Steps
24 g of 3,6-dimethylpyridazine and 60 g of p-nitrobenzenealdehyde are dissolved in one liter of acetic acid anhydride, which is heated and refluxed to obtain 33 g of 3,6-di(p-nitrostyryl)pyridazine (K').
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04871633 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-1fab1cbdde784f64b96bef37330626f9 |
| Source note | uspto-grants-1989_10 |