huagongshe.com
HRID2350838

反应详情

EQUATION

反应方程式

HRID 2350838 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc([N+](=O)[O-])cc1
HCID541

4-Nitrobenzaldehyde

C7H5NO3

结构：Cc1ccc(C)nn1
HCID527031

3,6-dimethylpyridazine

C6H8N2

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(C=Cc2ccc(C=Cc3ccc([N+](=O)[O-])cc3)nn2)cc1
HCID54059565

未命名化合物

收率 44.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)OC(C)=O
溶剂HCID7918

Acetic anhydride

C4H6O3

PROCEDURE

实验过程

24 g of 3,6-dimethylpyridazine and 60 g of p-nitrobenzenealdehyde are dissolved in one liter of acetic acid anhydride, which is heated and refluxed to obtain 33 g of 3,6-di(p-nitrostyryl)pyridazine (K').

WORKUP

后处理

  1. temperaturewhich is heated
  2. temperaturerefluxed