Ethyl Acrylate → HCID 52192718, compound

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Reaction Steps

25.0 g of 4-phenylpiperidine (0.15 mol) are placed in 50 ml of diethyl ether and, while stirring, 15.1 g of ethyl acrylate are gradually added thereto. With a slight increase in temperature, a clear solution forms. After standing overnight at room temperature, the ether is distilled off. The oil remaining behind is the crude 3-(4-phenylpiperidino)-propionic acid ethyl ester (yield approx. 95%).

Provenance & Evidence