HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351291Generated: October 31, 2026
(1,2-Dibromoethyl)benzene → HCID 13112855, compound
https://huagongshe.com/reaction/2351291
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (1,2-Dibromoethyl)benzene | HCID 7145 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13112855 | HCID 13112855 | — |
Reaction Steps
(1,2-Dibromoethyl)benzene (21 g) was treated with 2-mercaptobenzimidazole (17 g) in dimethylformamide (100 ml) and the mixture was heated at 100° C. for 36 hours. On cooling, the solid material was removed by filtration and recrystallised from methanol and ethyl acetate to give the title compound as the hydrobromide salt (13.68 g). mp 207°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04873237 |
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| Source dataset | uspto-grants-1989_10 |
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| ORD ID | ord-cf51b49fd2f94f11bc5e1f8209cb88e4 |
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| Source note | uspto-grants-1989_10 |
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