m-Chloroperbenzoic acid → HCID 19846103, compound

HRID 2351292Notes

Reaction equation

HRID 2351292 reaction equation
[CH3:1][C:2]1[C:3]([CH3:20])=[CH:4][C:5]2[N:9]=[C:8]3[S:10][CH:11]([C:13]4[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=4)[CH2:12][N:7]3[C:6]=2[CH:19]=1.ClC1C=C(C=CC=1)C(OO)=[O:26]>>[CH3:1][C:2]1[C:3]([CH3:20])=[CH:4][C:5]2[N:9]=[C:8]3[S:10](=[O:26])[CH:11]([C:13]4[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=4)[CH2:12][N:7]3[C:6]=2[CH:19]=1

Participants

3

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 19846091HCID 19846091, compound

Product 1

HCID 19846103HCID 19846103, compound

Procedure

In a manner analogous to Example 10 2,3-Dihydro-6,7-dimethyl-2-(2-pyridyl)thiazolo- [3,2-a]benzimidazole (2.63 g) was reacted with m-chloroperoxybenzoic acid (1.45 g) to give the title compound as the 1/4 hydrate, mp 177°-8° C. decomp.

Sources & evidence

ORD record
ord-01cb85c35373461283c2623a7ddacd36
Source dataset
uspto-grants-1989_10
Patent number
US04873237

Reaction notes

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