HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 3-(1-Piperidinylmethyl)-1-pyrrolidineacetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 19846039 | HCID 19846039 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | 3-(1-Piperidinylmethyl)-1-pyrrolidineacetonitrile | HCID 19846035 | — |
Reaction Steps
2-[3-[(dipropylamino)methyl]-piperidin-1-yl]acetonitrile in a yield of 76% of theory, RF 0.545 (Macherey-Nagel, PolygramRSIL G/UV254, pre-coated plastic sheets for TLC, eluant: dichloromethane/methanol/conc. ammonia 89/10/1 v/v);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-837849fa20a84a009c057d22333e1fba |
| Source note | uspto-grants-1989_10 |