Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351389Generated: November 1, 2026

Diisopropyl Ether → HCID 14210074, compound

https://huagongshe.com/reaction/2351389

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropyl EtherHCID 7914—
Reactant5-chlorocarbonyl-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-oneHCID 13276745—
Reactant2-[2-[(Diethylamino)methyl]piperidin-1-yl]ethanamineHCID 14210000—
ProductHCID 14210074HCID 1421007474%

Reaction Steps

Prepared analogously to Example 2 from 5-(chlorocarbonyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 2-[2-[(diethylamino)methyl]-piperidin-1-yl]-ethanamine in a yield of 74% of theory. Colourless crystals, m.p. 123°-125° C. (diisopropylether).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-9853fa857bbe4c71b89f07e6905732d7
Source noteuspto-grants-1989_10