HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 53925832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Reactant | HCID 14210026 | HCID 14210026 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 53925832 | HCID 53925832 | 62% |
Reaction Steps
Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[2-[(diethylamino)methyl]-piperidin-l-yl]-1,1-dimethyl-ethanamine in a yield of 62% of theory. Colourless crystals, m.p. 160°-162° C. (acetonitrile and ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-f301b755c7da491fa184b99b0263c528 |
| Source note | uspto-grants-1989_10 |