HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 19845924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Reactant | HCID 19846010 | HCID 19846010 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19845924 | HCID 19845924 | 34% |
Reaction Steps
Prepared analogously to Example 1 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[2-[[bis(methylethyl)amino]methyl]-piperidin-l-yl]ethanamine in a yield of 34% of theory. Colourless crystals, m.p. 181°-182° C. (acetonitrile using activated charcoal).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-73b6046a90f54c2292a8a878940c2d53 |
| Source note | uspto-grants-1989_10 |