Hydrochloric Acid → HCID 14181207, compound

HRID 2351469Notes

Reaction equation

HRID 2351469 reaction equation
[CH2:1]([N:4]([CH2:17][CH2:18][CH3:19])[CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([CH2:15][NH2:16])[CH:9]=[CH:10][CH:11]=2)[CH2:6]1)[CH2:2][CH3:3].[ClH:20]>CCOCC>[ClH:20].[CH2:17]([N:4]([CH2:1][CH2:2][CH3:3])[CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([CH2:15][NH2:16])[CH:9]=[CH:10][CH:11]=2)[CH2:6]1)[CH2:18][CH3:19]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 14181206HCID 14181206, compound

Product 1

HCID 14181207HCID 14181207, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The compound of Example 12 was dissolved in ether. By dropwise addition of ethereal hydrogen chloride solution, the hydrochloride was precipitated and was then filtered off under suction and dried in vacuo at room temperature.

Workup

  1. customthe hydrochloride was precipitated
  2. filtrationwas then filtered off under suction
  3. customdried in vacuo at room temperature

Sources & evidence

ORD record
ord-cf4575699f7240fa9ea02647c3132afa
Source dataset
uspto-grants-1989_10
Patent number
US04873262

Reaction notes

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