HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15613929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15671171 | HCID 15671171 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 15613929 | HCID 15613929 | 78.9% |
Reaction Steps
A procedure similar to that described in Example 15 was repeated, except that 1.1 g of ethyl 2-[4-(2,4-dioxothiazolidin-5-ylmethyl)phenoxymethyl]-2-methylchroman-6-carboxylate (prepared as described in Example 17), 10 ml of acetic acid and 5 ml of 3N aqueous hydrochloric acid were used, to afford 814 mg of the title compound as colorless crystals, melting at 223°-225° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873255 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-e6f9f81528fb45c188cfd51508e167c3 |
| Source note | uspto-grants-1989_10 |